Mps1-IN-1_LCMS_14736_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20150119\\20150119 2015-01-19 09-28-05\\BIZ2015-119-DJL6.DSample Name: BIZ2015-119-DJL6=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 66Acq. Instrument : HY-LCMS-02 Location : Vial 61Injection Date : 1/19/2015 3:04:50 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150119\\20150119 2015-01-19 09-28-05\\100-1000MS+3MIN( 0.02%FA).MLast changed : 1/19/2015 9:28:05 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\BLHM-342_45-H01P(RP-HPLC).MLast changed : 1/19/2015 4:05:14 PM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc Catalog No : HY-13298 Batch#14736 A-RP-124 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT...60\\DATA\\20150119\\20150119 2015-01-19 09-28-05\\BIZ2015-119-DJL6.D) 1.417 1.555mAU80060040020000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.417 MF 0.0471 2816.76392 996.85120 99.6112 2 1.555 FM 0.0453 10.99302 4.04049 0.3888 Totals : 2827.75694 1000.89168 ===================================================================== *** End of Report ***HY-LCMS-02 1/19/2015 4:05:15 PM Li Shan(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20150119\\20150119 2015-01-19 09-28-05\\BIZ2015-119-DJL6.DSample Name: BIZ2015-119-DJL6=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 66Acq. Instrument : HY-LCMS-02 Location : Vial 61Injection Date : 1/19/2015 3:04:50 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150119\\20150119 2015-01-19 09-28-05\\100-1000MS+3MIN( 0.02%FA).MLast changed : 1/19/2015 9:28:05 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\BLHM-342_45-H01P(RP-HPLC).MLast changed : 1/19/2015 4:06:43 PM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc Catalog No : HY-13298 Batch#14736 A-RP-124 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150119\\20150119 2015-01-19 09-28-05\\BIZ2015-119-DJL6.D) ES-API, Pos, Sca 1.407100000080000060000040000020000000.511.522.53min HY-LCMS-02 1/19/2015 4:06:44 PM Li Shan(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20150119\\20150119 2015-01-19 09-28-05\\BIZ2015-119-DJL6.DSample Name: BIZ2015-119-DJL6MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.407 5258181 537.20 I 536.20 I 268.60 I*MSD1 SPC, time=1.379:1.434 of D:\\AGLIENT 1260\\DATA\\20150119\\20150119 2015-01-19 09-28-05\\BIZ2015-119-DJL6.D ES-API,100806040200100200300400500m/z 268.6 536.2Max: 375024 *** End of Report ***HY-LCMS-02 1/19/2015 4:06:44 PM Li Shan(LCMS-02) 538.2 537.2Page 2 of 2